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荔枝皮化学成分的研究(Ⅰ)
关小丽, 黄永林, 刘春丽, 李典鹏
1. 广西植物功能物质研究与利用重点实验室, 广西植物研究所, 广西 桂林 541006;2. 广西中医药大学, 南宁 530001;3. 广西师范大学, 广西 桂林 541004
摘要:
采用Sephadex LH-20、MCI gel CHP 20P和Toyopearl Butly-650C等柱色谱,反复对80%乙醇荔枝皮提取物进行分离、纯化,得到7个多酚类化合物。根据波谱分析以及文献数据对比,分别鉴定为对羟基苯甲酸(1)、原儿茶酸(2)、(+)儿茶素(3)、(-)表儿茶素(4)、原花青素A2(5)、aesculitannin A(6)、槲皮素-3-O-β-D-葡萄糖苷(7)。除5以外的化合物均为首次从荔枝果皮中分离得到。
关键词:  荔枝皮  多酚类  化学成分
DOI:10.3969/j.issn.1000-3142.2014.02.003
分类号:Q946.8
Fund project:
Study on the chemical constituents of Litchi chinensis pericarp(1)
GUAN Xiao-Li1,2, HUANG Yong-Lin1, LIU Chun-Li1,3, LI Dian-Peng1*
1. Guangxi Key Laboratory of Functional Phytochemicals Research and Utilization, Guangxi Institute of Botany, Guilin 541006, China;2. Guangxi University of Chinese Medicine, Nanning 530001, China, 3. Guangxi Normal University, Guilin 541004, China
Abstract:
The 80% ethanol extracts of the Litchi chinensis pericarp was isolated and purified by Sephadex LH-20,MCI gel CHP 20P,Toyopearl Butly-650C column chromatography to yield seven phenolic compounds. Their structures were identified by the analysis of spectral data as:p-Hydroxybenzoic acid(1),3,4-dihydroxybenzoic acid(2),(+)-catechin(3),(-)-epicatechin(4),procyanidin A2(5),aesculitannin A(6),quercetin-3-O-β-D-glucopyranoside(7). All the compounds except 5 were reported from L. chinensis pericarp for the first time.
Key words:   Litchi chinensis pericarp  polyphenols  chemical constituents
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