蝴蝶果根、果仁挥发油化学成分的研究

苏秀芳<sup>1; 2</sup>; 林 强<sup>1*</sup>; 梁振益<sup>1</sup>; 杨先会<sup>1</sup>

引用本文:	苏秀芳, 林强, 梁振益, 杨先会.蝴蝶果根、果仁挥发油化学成分的研究[J].广西植物,2009,(2):281-283.[点击复制]
	SU Xiu-Fang, LIN Qiang, LIANG Zhen-Yi, YANG Xian-Hui.Study on the chemical constituent of essential oil from roots and nutlets of Cleidiocarpon cavaleriei[J].Guihaia,2009,(2):281-283.[点击复制]

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蝴蝶果根、果仁挥发油化学成分的研究
苏秀芳^1,2, 林强^1*, 梁振益¹, 杨先会¹
1.海南大学理工学院, 海口 570228;2.南宁师范高等专科学校化学与生物工程系, 广西龙州 532400

摘要:

采用水蒸气蒸馏法从大戟科蝴蝶果的根和果仁中提取挥发油,用气相色谱-质谱联用技术对挥发油化学成分进行分析,并应用面积归一化法测定各成分的相对百分含量。从根中鉴定出23种化合物,占总油量的100%,其主要成分为十六烷酸(18.74%)、(Z,Z)9,12-十八碳二烯酸(12.81%)、1,2-苯二羧酸双(2-甲基丙基)酯(10.59%)、二丁基邻苯二甲酸酯(7.42%)及二十四烷(6.72%)。从果仁中鉴定出17种化合物,占总油量的100%,主要成分为(E-)-9-十八碳烯酸(23.15%)、正十六烷酸(21.20%)、(Z,Z)-9,12-十八碳二烯酸(19.26%)及3-甲基十七烷(6.80%)。

关键词: 蝴蝶果挥发油气相色谱—质谱联用技术

DOI：

分类号:Q946.91

基金项目:

Study on the chemical constituent of essential oil from roots and nutlets of Cleidiocarpon cavaleriei

SU Xiu-Fang^1,2, LIN Qiang^1*, LIANG Zhen-Yi¹, YANG Xian-Hui¹

1.Hainan University, College of Science and Technology, Haikou 570228, China;2.Department of Chemistry and Biological Engineering, Nanning Normal High School, Longzhou 532400, China

Abstract:

The essential oil extracted from the roots and nutlets of Cleidiocarpon cavaleriei were analyzed by GC-MS for the first time. The relative contents were determined by area normalization. 23 compounds were identified,which accounted for 100% of the essential oil of the roots. The major compositions were n-Hexadecanoic acid(18.74%);(Z,Z)-9,12-Octadecadienoic acid(12.81%),1,2-Benzenedicarboxylic acid,bis(2-methylpropyl)ester(10.59%),Dibutyl phthalatephthalate(7.42%)and Tetracosane(6.72%). 17 compounds were identified,which accounted for 100% of the essential oil of the nutlets. The major compositions were(E)-9-Octadecenoic acid(23.15%),n-Hexadecanoic acid(21.20%),(Z,Z)-9,12-Octadecadienoic acid(19.26%)and 3-Methyl-heptadecane(6.80%).

Key words: Cleidiocarpon cavaleriei essential oil GC-MS