小果十大功劳化学成分的研究

张文芳<sup>1; 2</sup>; 李 涛<sup>2</sup>; 娄华勇<sup>2</sup>; 潘卫东<sup>2*</sup>

引用本文:	张文芳, 李涛, 娄华勇, 潘卫东.小果十大功劳化学成分的研究[J].广西植物,2014,(4):500-504.[点击复制]
	ZHANG Wen-Fang, LI Tao, LOU Hua-Yong, PAN Wei-Dong.Chemical constituents from Mahonia bodinieri[J].Guihaia,2014,(4):500-504.[点击复制]

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小果十大功劳化学成分的研究
张文芳^1,2, 李涛², 娄华勇², 潘卫东^2*
1. 贵阳中医学院, 贵阳 550002;2. 贵州省中国科学院天然产物化学重点实验室, 贵阳 550002

摘要:

从小果十大功劳的石油醚层、氯仿层、正丁醇层中分离出9个化合物,利用UV、IR、NMR和MS等现代波谱分析方法,鉴定这9个化合物的结构为:二十九烷-10-醇(1)、亚麻酸甲酯(2)、β-谷甾醇(3)、小檗碱(4)、异汉防已碱甲素(5)、四氢小檗碱(6)、白蓬皱褶碱(7),药根碱(8),1-棕榈酸单甘油酯(9)。所有化合物均为首次从该植物中分离得到。

关键词: 小果十大功劳化学成分结构鉴定

DOI：10.3969/j.issn.1000-3142.2014.04.014

分类号:

基金项目:

Chemical constituents from Mahonia bodinieri

ZHANG Wen-Fang^1,2, LI Tao², LOU Hua-Yong², PAN Wei-Dong^2*

1. Guiyang College of Traditional Chinese Medicine, Guiyang 550002, China;2. Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences, Guiyang 550002, China

Abstract:

The chemical constituents of Mahonia bodinieri were studied by the method of chromatography and spectral analysis. Nine compounds were isolated and identified as nonacosan-10-ol(1),methyllinolenate(2),β-sitosterol(3),berberine(4),isotetrandrine(5),tetrahydroberberine(6),thalrugosine(7),jatrorrhizine(8),1-monoplamitin(9). All these compounds were isolated from this genus for the first time.

Key words: Mahonia bodinieri chemical constituent structural elucidation