刺山柑果实中硫单质的分离与晶体结构

李海军1; 2; $21; 2*; $23; $21; 2

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刺山柑果实中硫单质的分离与晶体结构
李海军1，2，白红进1，2*，张继文3，王安银1，2
1.新疆生产建设兵团塔里木盆地生物资源保护利用重点实验室，新疆阿拉尔 843300;2.塔里木大学 生命科学学院，新疆阿拉尔 843300;3.西北农林科技大学理学院，陕西杨凌 712100

摘要:

从刺山柑果实中首次分离纯化得到S8单质。经X 射线单晶衍射分析，确认该化合物为S8晶体，M=256.48。晶体属斜方晶系，空间群Fddd。晶胞参数a=10.456(7)，b=12.908(9)，c=24.483(17)，V=3305(4)3，Z=16，F(000)=2048，R1=0.0915，wR2=0.1820。

关键词: 刺山柑硫单质 X 射线单晶衍射晶体结构

DOI：

分类号:R284.2；O723

Fund project:

Isolation and crystal ctructure of sulfur from Capparis spinosa fruits

LI HaiJun1，2， BAI HongJin1，2*， ZHANG JiWen3， WANG AnYin1，2

1.Key Laboratory of Protection and Utilization of Biological Resources in Tarim Basin， Xinjiang Prodution and Construction Corps， Alar 843300， China;2.College of Life Sciences， Tarim University， Alar 843300， China;3.College of Sciences， Northwest A & F University， Yangling 712100， China

Abstract:

The purpose of this paper studied single crystal structure of S8 isolated firstly from Capparis spinosa fruits. The S8 crystal structure was investigated by single crystal X ray crystallographic analysis crystallizes in the monoclinic system，M=256.48.space group Fddd. Unit cell parameters a=10.456(7)，b=12.908(9)，c=24.483(17)，V=3305(4)3，Z=16，F(000)=2048. The final R1=0.0915，wR2=0.1820.

Key words: Capparis spinosal element sulfur single crystal X ray diffraction crystal structure