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红树白骨壤果实中酚苷类化学成分研究
谢文佩1, 高程海2, 易湘茜1*, 易 蔚1, 何碧娟2, 陈 波2
1. 广西中医药大学 药学院, 南宁 530001;2. 广西科学院 广西近海海洋环境科学重点实验室, 南宁 530007
摘要:
采用柱色谱、凝胶层析和高效液相色谱分离技术,从白骨壤果实中分离获得6个酚苷类单体化合物。运用波谱分析和文献对照方法,分别鉴定为Rhyncoside A(1)、松柏苷(2)、对羟基苯甲酰葡萄糖(3)、顺式香豆酸-4-O-β-D-吡喃葡萄糖苷(4)、香草酸4-O-β-D-吡喃葡萄糖苷(5)、苯基-β-D-葡萄糖苷(6)。化合物1-6均是首次从该种海洋植物中分离得到。
关键词:  白骨壤  果实  酚苷类化合物  结构鉴定
DOI:10.3969/j.issn.1000-3142.2014.03.021
分类号:Q946.91
Fund project:
Study on phenolic glycosides from fruit of the mangrove plant Avicennia marina
XIE Wen-Pei1, GAO Cheng-Hai2, YI Xiang-Xi1*, YI Wei1, HE Bi-Juan2, CHEN Bo2
1. Faculty of Pharmacy, Guangxi University of Chinese Medicine, Nanning 530001, China;2. Guangxi Key Laboratory of Marine Environmental Science, Guangxi Academy of Sciences, Nanning 530007, China
Abstract:
Six phenolic glycosides were isolated by silica gel column chromatography,PTLC,and semi-preparative HPLC from the fruit of Avicennia marina. By means of spectroscopic analysis and comparison with literatures,their compounds were identified as Rhyncosides A(1),Coniferin(2),l-(4-Hydorxybenzoyl)-glucose(3),(Z)-4-Coumaric acid 4-O-β-D-glucopyranoside(4),Vanillic acid 4-O-β-D-glucopyranoside(5),Phenyl-β-D-glucopyranoside(6). All compounds were isolated from this plant for the first time.
Key words:  Avicennia marina  fruit  phenolic glycosides  structure identification
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